Paper · 2020 · Butlerov Communications

Quantitative determination of the total content γ-pyrone Compounds in the aerial part of Halenia corniculata by HPLC

Tatiana M. Shishmareva

15
claims
30
verbatim quotes
0
citations
1
research areas
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Open access

Abstract

This work presents the results of a quantitative determination of the total content of γ-pyrone compounds in the aerial part of Halenia corniculata using the HPLC method, where the standard samples of 1-hydroxy-2,3,5-trimethoxyxanthone and 1-hydroxy-2,3,4,5-tetramethoxyxanthone. The main active ingredients of H. corniculata are xanthones and flavones, and this plant can be used as a possible source of available phenol compounds. To determine the total content of xanthones and flavones in the aerial part of H. corniculata, the hexane, chloroform, and ethyl acetate fractions were studied. During the experiment, 13 compounds were found in the hexane fraction of H. corniculata, among which the content of 1-hydroxy-2,3,4,5-tetramethoxyxanthone is 43.07% of the mass of the hexane fraction and 1.44% of the mass of absolutely dry raw materials, and 1-hydroxy-2,3,5-trimethoxyxanthone – 22.20% by weight of the hexane fraction and 0.74% by weight of absolutely dry raw materials. In the chloroform fraction of H. corniculata, 17 compounds were found, and 1-hydroxy-2,3,4,5-tetramethoxyxanthone (6.26% of the mass of the chloroform fraction and 0.20% of the mass of absolutely dry raw materials) and 1-hydroxy-2,3,5-trimethoxyxanthone (4.22% by weight of the chloroform fraction and 0.13% by weight of absolutely dry raw materials). In the study of the ethyl acetate fraction of H. corniculata, 14 compounds were found, among which 1 component was identified – luteolin, the content of which is 68.26% of the weight of the ethyl acetate fraction and 2.41% of the weight of absolutely dry raw material. The total content of γ-pyrone compounds in the aerial part of H. corniculata is 4.92% (based on the weight of the absolute dry raw material).

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Claims 15

Observationobservedoriginal resultmeasured

Claim · model-written summary

The total content of gamma-pyrone compounds in the aerial part is 4.92% of dry raw material.

Taxon
Halenia corniculataHalenia corniculatat0
Organ / stage
aerial parte1
Outcome
total content of γ-pyrone compoundse1
Value
4.92%e1
Qualifier
based on the weight of the absolute dry raw materiale1

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e1

“The total content of γ-pyrone compounds in the aerial part of H. corniculata is 4.92% (based on the weight of the absolute dry raw material)”

✓ located verbatim in the source · abstract, characters 1604–1744 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

Thirteen compounds were found in the hexane fraction.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
compounds were founde2
Value
13e2
Qualifier
hexane fractione2

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e2

“During the experiment, 13 compounds were found in the hexane fraction of H. corniculata”

✓ located verbatim in the source · abstract, characters 594–681 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,4,5-tetramethoxyxanthone was 43.07% of the hexane fraction mass.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,4,5-tetramethoxyxanthonee3
Value
43.07%e3
Qualifier
of the mass of the hexane fractione3

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e3

“the content of 1-hydroxy-2,3,4,5-tetramethoxyxanthone is 43.07% of the mass of the hexane fraction and 1.44% of the mass of absolutely dry raw materials”

✓ located verbatim in the source · abstract, characters 695–847 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,4,5-tetramethoxyxanthone was 1.44% of the dry raw material mass.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,4,5-tetramethoxyxanthonee3
Value
1.44%e3
Qualifier
of the mass of absolutely dry raw materialse3

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e3

“the content of 1-hydroxy-2,3,4,5-tetramethoxyxanthone is 43.07% of the mass of the hexane fraction and 1.44% of the mass of absolutely dry raw materials”

✓ located verbatim in the source · abstract, characters 695–847 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,5-trimethoxyxanthone was 22.20% of the hexane fraction by weight.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,5-trimethoxyxanthonee4
Value
22.20%e4
Qualifier
by weight of the hexane fractione4

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e4

“1-hydroxy-2,3,5-trimethoxyxanthone – 22.20% by weight of the hexane fraction and 0.74% by weight of absolutely dry raw materials”

✓ located verbatim in the source · abstract, characters 853–981 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,5-trimethoxyxanthone was 0.74% of the dry raw material by weight.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,5-trimethoxyxanthonee4
Value
0.74%e4
Qualifier
by weight of absolutely dry raw materialse4

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e4

“1-hydroxy-2,3,5-trimethoxyxanthone – 22.20% by weight of the hexane fraction and 0.74% by weight of absolutely dry raw materials”

✓ located verbatim in the source · abstract, characters 853–981 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

Seventeen compounds were found in the chloroform fraction.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
compounds were founde5
Value
17e5
Qualifier
chloroform fractione5

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e5

“In the chloroform fraction of H. corniculata, 17 compounds were found”

✓ located verbatim in the source · abstract, characters 983–1052 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,4,5-tetramethoxyxanthone was 6.26% of the chloroform fraction mass.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,4,5-tetramethoxyxanthonee6
Value
6.26%e6
Qualifier
of the mass of the chloroform fractione6

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e6

“1-hydroxy-2,3,4,5-tetramethoxyxanthone (6.26% of the mass of the chloroform fraction and 0.20% of the mass of absolutely dry raw materials)”

✓ located verbatim in the source · abstract, characters 1058–1197 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,4,5-tetramethoxyxanthone was 0.20% of the dry raw material mass in the chloroform study.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,4,5-tetramethoxyxanthonee6
Value
0.20%e6
Qualifier
of the mass of absolutely dry raw materialse6

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e6

“1-hydroxy-2,3,4,5-tetramethoxyxanthone (6.26% of the mass of the chloroform fraction and 0.20% of the mass of absolutely dry raw materials)”

✓ located verbatim in the source · abstract, characters 1058–1197 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,5-trimethoxyxanthone was 4.22% of the chloroform fraction by weight.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,5-trimethoxyxanthonee7
Value
4.22%e7
Qualifier
by weight of the chloroform fractione7

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e7

“1-hydroxy-2,3,5-trimethoxyxanthone (4.22% by weight of the chloroform fraction and 0.13% by weight of absolutely dry raw materials)”

✓ located verbatim in the source · abstract, characters 1202–1333 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

1-hydroxy-2,3,5-trimethoxyxanthone was 0.13% of the dry raw material by weight in the chloroform study.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
1-hydroxy-2,3,5-trimethoxyxanthonee7
Value
0.13%e7
Qualifier
by weight of absolutely dry raw materialse7

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e7

“1-hydroxy-2,3,5-trimethoxyxanthone (4.22% by weight of the chloroform fraction and 0.13% by weight of absolutely dry raw materials)”

✓ located verbatim in the source · abstract, characters 1202–1333 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

Fourteen compounds were found in the ethyl acetate fraction.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
compounds were founde1
Value
14e1
Qualifier
ethyl acetate fractione1

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e1

“In the study of the ethyl acetate fraction of H. corniculata, 14 compounds were found”

✓ located verbatim in the source · abstract, characters 1335–1420 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

Luteolin was 68.26% of the ethyl acetate fraction by weight.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
luteoline1
Value
68.26%e1
Qualifier
of the weight of the ethyl acetate fractione1

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e1

“1 component was identified – luteolin, the content of which is 68.26% of the weight of the ethyl acetate fraction and 2.41% of the weight of absolutely dry raw material”

✓ located verbatim in the source · abstract, characters 1434–1602 · show in text ↑
Observationobservedoriginal resultmeasured

Claim · model-written summary

Luteolin was 2.41% of the dry raw material weight.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
luteoline1
Value
2.41%e1
Qualifier
of the weight of absolutely dry raw materiale1

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e1

“1 component was identified – luteolin, the content of which is 68.26% of the weight of the ethyl acetate fraction and 2.41% of the weight of absolutely dry raw material”

✓ located verbatim in the source · abstract, characters 1434–1602 · show in text ↑
Recommendationauthor interpretationoriginal resultbasis n/a

Claim · model-written summary

Halenia corniculata can be a possible source of available phenol compounds.

Taxon
Halenia corniculataHalenia corniculatat0
Outcome
source of available phenol compoundse2

Organisms pictured · Representative pictures of the matched species, not figures from the paper.

Halenia corniculata
Halenia corniculata · TaxonQwert1234 · CC BY-SA 3.0 · Wikimedia Commons ↗

Verbatim

t0

“Halenia corniculata”

✓ located verbatim in the source · title, characters 89–108 · show in text ↑
e2

“this plant can be used as a possible source of available phenol compounds”

✓ located verbatim in the source · abstract, characters 358–431 · show in text ↑